Effect Of Sonication Conditions Solvent Time Temperature

Influence of ultrasonic amplitude, temperature, time and solvent …

A four factors, three levels Box-Behnken design was adapted in this study to investigate and optimize the effect of the independent variables – ultrasonic amplitude (X 1), ethanol concentration (X 2), temperature (X 3) and time (X 4) – on the balsam, TPC and TFC.The coded levels of the variables are shown in Table 1.All calculations and …

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Processes | Free Full-Text | D-Limonene as a Promising Green Solvent …

The effects of sonication power, thermal pre-treatment, temperature, and contact time on detachment percentage were examined, and the best conditions (namely, no pre-treatment, medium sonication power of 450 W, temperature of 60 °C, and a contact time of 120 min) were found for total component detachment.

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Effect of sonication conditions: solvent, time and …

This paper describes the effect of temperature, time, solvent and sonication conditions under air and Argon for the preparation of micron and sub-micron sized vermiculite …

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(PDF) Effect of sonication conditions: Solvent, time, …

The sonication promoted also the preferential dissolution of the Na+ exchangeable cations due to the delamination and further separation of the clay mineral layers. The …

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Effect of Time, Solvent-Solid Ratio, Ethanol Concentration …

Based on experimental results, the optimum raw materials to solvent ratio was 1:30, solvent concentration was 70%, extraction temperature was 50°C, ultrasonic power was 60% and extraction time ...

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Effect of sonication conditions: Time, temperature and …

The influence of sonication conditions (amplitude of ultrasound probe = 50, and 75%, time = 5, 10 and 15 min and temperature = 45, 55 and 65 °C) on the properties of yoghurt was investigated ...

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Effect of sonication conditions: solvent, time and …

This paper describes the effect of temperature, time, solvent and sonication conditions under air and Argon for the preparation of micron and sub-micron sized vermiculite particles in a Rosett-type reactor. The resulting material were characterized via X-ray powder diffraction (XRDP),

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Modeling the effect of sonication parameters on size and …

The objective of this study was to evaluate the effect of sonication time and pulse frequency on average dispersion temperature (ART), particle size and zeta potential of solid lipid nanoparticles ...

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Effect of sonication conditions: solvent, time, temperature …

Effect of sonication conditions: solvent, time, temperature and reactor type on the preparation of micron sized vermiculite particles. (PMID:24262759) PMID:24262759

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Effect of sonication on particle dispersion, administered …

The effect of sonication time on the particle size distribution will therefore be presented for stock solutions with particle concentrations of 1 g/L. The extension of the sonication time (delivered acoustic energy) from 3 (180 s) to 15 min (882 s) resulted in the disintegration of larger agglomerates into units of smaller size for the Cu, Mn ...

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Effect of sonication conditions: Time, temperature and …

The influence of sonication conditions (amplitude of ultrasound probe = 50, and 75%, time = 5, 10 and 15 min and temperature = 45, 55 and 65 ºC) on the properties of yoghurt was investigated. The apparent viscosity, hardness and lightness increased when sonication time, temperature and amplitude increased.

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A review on possible mechanisms of sonocrystallisation in …

However, the effects of mixing are different from the effects induced by US, with the crystals obtained under sonicated conditions being superior in terms of uniformity with respect to size and shape [14], [73], [85], as it is shown in Fig. 5. Crystals obtained with sonication are more regular, and no agglomeration has been detected.

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(PDF) Effect of sonication conditions: Solvent, time, …

The effects of temperature, time, solvent and sonication conditions under air and Argon are described for the preparation of micron and sub-micron sized vermiculite particles in a...

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Sonication amplitude and processing time influence the …

The bubbles breakdown, which is called cavitation, creates dramatic effects in the sonicated liquid and give rise to pressures up to 1000 atm and temperatures of up to 5000 K [Citation 11].Acoustic cavitation impact is strong enough to split up the fine particle agglomerates and disperse them more uniformly in liquids [Citation 12].In the …

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Effect of sonication time on the evaporation rate of …

Sonication time effect on evaporation rate of GNP@MWCNT nanofluid was investigated. • Optimum sonication time was obtained at 120 min with 61.3% evaporation efficiency. • Effect of nanoparticle mass fraction and irradiation on efficiency was studied. • GNP@MWCNT nanofluid at 120 min sonication showed the best cost-efficiency. •

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(PDF) Effect of sonication conditions: Solvent, time, temperature …

Effect of sonication conditions: Solvent, time, temperature and reactor type on the preparation of micron sized vermiculite particles

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The effects of temperature, time, solvent and sonication conditions under air and Argon are described for the preparation of micron and sub-micron sized vermiculite particles in a...

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Sonoluminescence intensity and ultrasonic cavitation temperature …

During sonication, the solvent and decomposition products volatilized, thereby lowering the specific heat ratio and average temperature in the bubble. When the vapor pressure is extremely low, the solvent does not volatilize into the cavitation, so the obtained average temperature was assumed to be the cavity temperature without …

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(PDF) EFFECT OF TEMPERATURE AND …

The influence of several parameters on the extraction of Labisia pumila were investigated : extraction time (1-8 hours), temperature (40,50,60, and 80 °C), and sonication (40% duty cycle …

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The effects of temperature, time, solvent and sonication conditions under air and Argon are described for the preparation of micron and sub-micron sized vermiculite particles in a double-jacketed ...

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Effect of sonication on particle dispersion, administered

The effect of sonication time on the particle size distribution will therefore be presented for stock solutions with particle concentrations of 1 g/L. The extension of the sonication time (delivered acoustic energy) from 3 (180 s) to 15 min (882 s) resulted in the disintegration of larger agglomerates into units of smaller size for the Cu, Mn ...

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Sonication: An overview

Ultrasonication produces radicals as a result of critical temperature and pressure conditions, which are responsible for dietary component alterations. ... Sonication is a time-consuming method that is only suitable for small batches. ... Effect of solvent composition and its interaction with ultrasonic energy on the ultrasound-assisted ...

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D-Limonene as a Promising Green Solvent for the …

The effects of sonication power, thermal pre-treatment, temperature, and contact time on detachment percentage were examined, and the best conditions (namely, no pre-treatment, medium sonication power of 450 W, temperature of 60 C, and a contact time of 120 min) were found for total component detachment. Additionally, the

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Effect of sonication conditions: Solvent, time, temperature …

Sonication promotes the dissolution of Na exchangeable cations through exfoliation. Improved exfoliation by sonication at 90°C in water or at room temperature in …

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Effect of sonication conditions: Time, temperature and …

DOI: 10.1111/1471-0307.12761 Corpus ID: 233836141; Effect of sonication conditions: Time, temperature and amplitude on physicochemical, textural and sensory properties of yoghurt

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Study of sonication parameters on PLA nanoparticles …

The Box-Behnken design improves and optimizes the polymeric nanoparticle preparation conditions using a simple emulsion-solvent evaporation technique. ... mean particle size for dispersions prepared at cycles of 20 s sonication time to 10%, 20%, and 30% of power, (B) PDI for dispersions prepared at cycles of 20 s sonication time to …

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Mastering The Art Of Sonication: A Step-By-Step Guide

Running the sonication process according to the selected parameters: Start the sonication process and monitor the progress closely. Maintain a consistent sonication environment by keeping the temperature and other conditions stable. Follow the recommended sonication time and power settings for your specific sample.

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Effect of sonication conditions: solvent, time, temperature …

Key takeaway: 'The efficiency of ultrasound irradiation on preparing micron-sized vermiculite particles is significantly affected by temperature, solvent, gas type, and reactor type.'

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(PDF) The effects of time, temperature, solvent: Solid ratio …

The effects of time, temperature, solvent: Solid ratio and solvent composition on extraction of total phenolic compound from dried olive (Olea europaea L.) leaves January 2010 35(6):411-416

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Ultrasound assisted extraction (UAE) of bioactive …

Whereas the negative linear effect of time on yield has been reported for pectin from sour orange peel, phenolic compounds from coconut (Cocos nucifera) shell powder in the time range 20–60 min . For the extraction of oil from papaya seed the yield increased with time at high temperature and high solvent to solid ratio . For the …

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